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Four-Ball Wear

ASTM D4172

40kg load, 1200 rpm, 1 hour @ 75°C — average wear scar across candidate blends in 50ml Formula Shell 5W-30.

  • 401Y blend0.33mm
  • 701Y blend0.41mm
  • 801Y blend0.43mm
  • 401Z blend0.43mm
  • 701Z blend0.43mm

Lab #23020231–23020235, tested May 2023.

Foaming Characteristics

ASTM D892

Sequence II @ 93.5°C, 5-minute aeration — foam volume with and without additive.

65mlbase oil only
50ml2.5ml/500ml (0.5%)

Sequences I & III (24°C) measured 0ml in every case, and all foam fully settles within 10 minutes. Lab #23020239a / #23020228.

Oxidation Stability

ASTM D6186 (PDSC)

Oxidation induction time at 210°C.

Base oil: 37.5 min+0.5% additive: 35.4 min

Stability stays in the same band after treatment — no significant loss of oxidative resistance. Lab #23020239c.

Full data table

Every sample,
every result

SampleTestMethodResultLab #
Formula Shell 5W-30 (base oil)Kinematic Viscosity @ 40°CD44564.51 cSt23020239
Formula Shell 5W-30 (base oil)Kinematic Viscosity @ 100°CD44510.92 cSt23020239
Formula Shell 5W-30 (base oil)Viscosity IndexD227016123020239
0.25ml 401X in 50ml base oil (0.5%)Kinematic Viscosity @ 40°CD44564.79 cSt23020239b
0.25ml 401X in 50ml base oil (0.5%)Kinematic Viscosity @ 100°CD44510.88 cSt23020239b
0.25ml 401X in 50ml base oil (0.5%)Viscosity IndexD227016023020239b
Formula Shell 5W-30 (base oil)Foam, Sequence II @ 93.5°CD89265 ml23020239a
2.5ml 401X in 500ml base oil (0.5%)Foam, Sequence II @ 93.5°CD89250 ml23020228
Formula Shell 5W-30 (base oil)Oxidation Induction @ 210°CD618637.5 min23020239c
0.25ml 401X in 50ml base oil (0.5%)Oxidation Induction @ 210°CD618635.4 min23020239c
0.5ml 401Y in 50ml base oilFour-Ball Wear ScarD41720.33 mm23020231
0.5ml 701Y in 50ml base oilFour-Ball Wear ScarD41720.41 mm23020232
0.5ml 801Y in 50ml base oilFour-Ball Wear ScarD41720.43 mm23020233
0.5ml 401Z in 50ml base oilFour-Ball Wear ScarD41720.43 mm23020234
0.5ml 701Z in 50ml base oilFour-Ball Wear ScarD41720.43 mm23020235
Test facility — Petro-Lubricant Testing Laboratories, Inc., 116 Sunset Inn Road, Lafayette, NJ 07848 Microscopy — A*STAR Institute of Materials Research and Engineering, Singapore Full reports — available on request via our contact page